STUDY THE EFFECT OF ZIRCONIUM, NICKEL AND HEAT-TREATMENTS ON THE MICROSTRUCTURE AND MECHANICAL PROPERTIES OF COLD-ROLLED AA6111 ALLOY

Authors

  • Saba Jameel Hassan Department of Metallurgical Engineering, Materials Engineering College, Babylon, University, Babil, Iraq
  • Basem Al-Zubaidy Department of Metallurgical Engineering, Materials Engineering College, Babylon, University, Babil, Iraq https://orcid.org/0000-0001-7699-1128
  • Saad Hameed Al-Shafaie Department of Metallurgical Engineering, Materials Engineering College, Babylon, University, Babil, Iraq

DOI:

https://doi.org/10.30572/2018/KJE/160110

Keywords:

AA6111 aluminum alloy, Al-Mg-Si-Zr-Ni alloys, Cold rolling, Artificial aging, Tensile properties

Abstract

The cold rolling effect on the microstructure and mechanical properties of recycled AA6111 alloy with Zr or/and Ni were investigated. All alloys were produced by the stir-casting method. homogenization heat treatment (500 ºC for 6 hours) was performed on AA6111 alloy only. The alloys were solutionized (at 540 ºC for 30 minute) and artificially aged (at 180 ºC for 10 hours). The optical micrograph, scanning-electron microscope (SEM) and X-ray Diffraction (XRD) studies for all samples. The microstructure analysis displayed different fine intermetallic phases distributed in large amounts in alloys containing Zr or/and nickel compared to AA6111 alloy. The combined alloying elements' addition effect with the cold rolling effect and artificial aging led to great improvements in the mechanical properties, where the hardness and tensile properties of all alloys increased. The AA6111+0.41wt%Ni alloy showed the highest hardness value, as it increased to 161 HV after artificial aging, while the AA6111+0.54wt%Zr alloy showed the highest YS and UTS, which increased to 252 MPa and 342 MPa, respectively.

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References

Akkar, A. Y., and Alali, M. (2023). 'Resistance spot welding of dissimilar metals AISI 1006 low carbon steel and AA6061 aluminum alloy using zing and tin coating'. Kufa Journal of Engineering, 14(3), 1-16. DOI: https://doi.org/10.30572/2018/KJE/140301

Al-Helal, K., Patel, J. B., and Fan, Z. (2020) 'Fe-rich intermetallic formation and mechanical properties of recycled AA6111 alloy strips produced by melt conditioning twin roll casting', Journal of JOM, 72(11), 3753-3759. DOI: https://doi.org/10.1007/s11837-020-04324-z

Al-Zubaidy, B. M. M. (2017) 'Material interactions in novel refill friction stir spot welding approach to join Al-Al and Al-Mg automotive sheets', The University of Manchester (United Kingdom).

Babaniaris, S., Ramajayam, M., Jiang, L., Langan, T., and Dorin, T.(2020) 'Tailored precipitation route for the effective utilization of Sc and Zr in an Al-Mg-Si alloy', Materialia, 10, 100656. DOI: https://doi.org/10.1016/j.mtla.2020.100656

Cahn, R. W., & Haasen, P. (Eds.). (1996) , Physical metallurgy (Vol. 1). Elsevier.

Chen, G., Kai, X., Tao, R., Cao, R., Qian, W., and Zhao, Y. (2023) 'Microstructure evolution and high-temperature performances of AA6111 alloy strengthened by Sc, Zr co-microalloying', Materials science and engineering journal, A, 887, 145788. DOI: https://doi.org/10.1016/j.msea.2023.145788

Dang, J. Z., Huang, Y. F., and Cheng, J. (2009) 'Effect of Sc and Zr on microstructures and mechanical properties of as-cast Al-Mg-Si-Mn alloys', Journal of transactions of nonferrous metals society of china, 19(3), 540-544. DOI: https://doi.org/10.1016/S1003-6326(08)60309-X

Djukanovic, G. (2019) 'Aluminum Alloys in the Automotive Industry: A Handy Guide', Journal of Aluminum Insider.

G. E. Totten and D. S. MacKenzie. (2003) 'Handbook of Aluminum, vol. 1, physical metallurgy and processes, vol. 1', CRC Press.

Hatch, J. E. (1984) 'Aluminium Properties and Physical Metallurgy', American Society for Metals.

Hetzner, D. W. (2003) 'Microindentation hardness testing of materials using ASTM E384' Microscopy and microanalysis journal, 9(S02), 708-709. DOI: https://doi.org/10.1017/S1431927603443547

Jiao, L., Wang, B., Zhao, Y., Wang, K., Li, F., and Li, H. (2023) 'Microstructure and plastic instability of (ZrB2+ Al3Zr)/AA6016 composites prepared by melt reaction method', Journal of materials engineering and performance, 32(5), 2509-2521. DOI: https://doi.org/10.1007/s11665-022-07271-9

Kang, S. B., Min, B. K., Kim, H. W., Wilkinson, D. S., and Kang, J. (2005) 'Effect of asymmetric rolling on the texture and mechanical properties of AA6111-aluminium sheet', Metallurgical and materials transactions journal A, 36, 3141-3149. DOI: https://doi.org/10.1007/s11661-005-0085-4

Mikhaylovskaya, A. V., Ghayoumabadi, M. E., and Mochugovskiy, A. G.(2021) 'Superplasticity and mechanical properties of Al-Mg-Si alloy doped with eutectic-forming Ni and Fe and dispersoid-forming Sc and Zr elements', Materials Science and Engineering, A, 817, 141319. DOI: https://doi.org/10.1016/j.msea.2021.141319

Mondolfo, L.F. (1976) 'Aluminium Alloys: Structure and Properties', Butterworths and Co., Ltd., London, 806. DOI: https://doi.org/10.1016/B978-0-408-70932-3.50404-6

Mukhopadhyay, P. (2012) 'Alloy designation, processing, and use of AA6XXX series aluminum alloys', International scholarly research notices. DOI: https://doi.org/10.5402/2012/165082

Okayasu, M., Sato, R., Takasu, S., Niikura, A., and Shiraishi, T. (2012) 'Mechanical properties of AlSiCu alloys produced by the twin rolled continuous casting process', Journal of materials science and engineering, A,534, 614-623 DOI: https://doi.org/10.1016/j.msea.2011.12.018

Qian, W., Kai, X., Tao, R., Gao, X., Huang, L., and Zhao, Y. (2023) 'The correlation between creep resistance and microstructure in AA6111 alloy strengthened by synergistic Er, Zr addition', Materials science and engineering journal, A, 870, 144867. DOI: https://doi.org/10.1016/j.msea.2023.144867

Quainoo, G. K., and Yannacopoulos, S. (2004) 'The effect of cold work on the precipitation kinetics of AA6111 aluminum', Journal of materials science, 39, 6495-6502. DOI: https://doi.org/10.1023/B:JMSC.0000044888.01854.e1

Quainoo, G. K., Yannacopoulos, S., and Gupta, A. K. (2001) 'Strengthening characteristics of AA6111 aluminum', Canadian metallurgical quarterly journal, 40(2), 211-220. DOI: https://doi.org/10.1179/000844301794388515

Raji, A. O., and Oke, S. A. (2020). 'Optimization of EDM for AA6061/10% Al2o3 AMMC using taguchi schemes and analytical hierarchy process for weight determination'. Kufa Journal of Engineering, 11(3). DOI: https://doi.org/10.30572/2018/KJE/110304

Sarkar, J., Kutty, T. R. G., Wilkinson, D. S., Embury, J. D., and Lloyd, D. J. (2004) 'Tensile properties and bendability of T4 treated AA6111 aluminum alloys', Materials science and engineering journal, A, 369(1-2), 258-266. DOI: https://doi.org/10.1016/j.msea.2003.11.022

Shurkin, P., Scamans, G., Barekar, N., Hou, L., Subroto, T., and Barbatti, C. (2023) 'Phase Composition and Microstructure of High Strength AA6xxx Aluminium Alloys with Nickel Additions', Materials transactions journal, 64(2), 398-405. DOI: https://doi.org/10.2320/matertrans.MT-LA2022047

Standard, A. S. T. M. (2012), E407-07 'Standard Practice for Microetching Metals and Alloys', ASTM International., West conshohocken, PA, 1-21

Xiao, Q., Liu, H., Yi, D., Yin, D., Chen, Y., Zhang, Y., and Wang, B. (2017) 'Effect of Cu content on precipitation and age-hardening behavior in Al-Mg-Si-xCu alloys', Journal of alloys and compounds, 695, 1005-1013. DOI: https://doi.org/10.1016/j.jallcom.2016.10.221

Zeren, M. (2005) 'Effect of copper and silicon content on mechanical properties in Al–Cu–Si–Mg alloys', Journal of materials processing technology, 169(2), 292-298. DOI: https://doi.org/10.1016/j.jmatprotec.2005.03.009

Zhang, L., Wang, Y., Yang, X., Li, K., Ni, S., Du, Y., and Song, M. (2017) 'The texture, microstructure, and mechanical properties of 6111 aluminum alloy are subject to rolling deformation', Materials research journal,20, 1360-1368. DOI: https://doi.org/10.1590/1980-5373-mr-2017-0549

Zhang, S., Xiong, B., Zhang, Y., Li, X., Wang, F., Li, Z., and Liu, H. (2013) 'The Microstructural Evolution of AA6111 Aluminium Alloy during Homogenization Treatment', In materials science forum (Vol. 749, pp. 223-228). DOI: https://doi.org/10.4028/www.scientific.net/MSF.749.223

Zhen, L., Fei, W. D., Kang, S. B., and Kim, H. W. (1997) 'Precipitation behavior of Al-Mg-Si alloys with high silicon content', Journal of materials science, 32, 1895-1902 DOI: https://doi.org/10.1023/A:1018569226499

Zuo, L., Ye, B., Feng, J., Zhang, H., Kong, X., and Jiang, H. (2020) 'Effect of ε-Al3Ni phase on mechanical properties of Al-Si–Cu–Mg–Ni alloys at elevated temperature', Journal of materials science and engineering: A, 772, 138794. DOI: https://doi.org/10.1016/j.msea.2019.138794

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Published

2025-02-04

How to Cite

Jameel Hassan, Saba, et al. “STUDY THE EFFECT OF ZIRCONIUM, NICKEL AND HEAT-TREATMENTS ON THE MICROSTRUCTURE AND MECHANICAL PROPERTIES OF COLD-ROLLED AA6111 ALLOY”. Kufa Journal of Engineering, vol. 16, no. 1, Feb. 2025, pp. 160-76, https://doi.org/10.30572/2018/KJE/160110.

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